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We actually do know the effect of breathing nitrogen gas. It's a hell of a lot better than injecting someone with a drug cocktail. I don't agree with the death penalty but this is about as humane as the death penalty gets.
Do you know that your body behaves differently when voluntarily being underwater while holding your breath and being held underwater while holding your breath knowing the person isn't going to let you breath again?
The negative side effects of the latter kick in way before you start to run out of oxygen.
That's not how it works. Your body can't detect a lack of oxygen but only build up of CO2. If you replace the air you breath with pure Helium, N2, CO, etc. you will just painlessly black out and die.
The difference is that nitrogen is odorless and colorless and we breath it in constantly. You won't notice it, you'll just start panting, get loopy, then lose consciousness.
That is relevant when the person doesn't know. Someone being executed will know that getting loopy means they are dying, and trigger a distress response.
CO2 isn't necessary to let your body know it is suffocating when you already know you are suffocating.
Starting to sound like your opinion to be honest. By the time he notices he's loopy, it is over.